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Gas chromatography and mass spectrometry of some trimethylsilyl derivatives of urinary glucuronides

✍ Scribed by J.E. Mrochek; W.T. Rainey Jr.

Publisher
Elsevier Science
Year
1974
Tongue
English
Weight
839 KB
Volume
57
Category
Article
ISSN
0003-2697

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πŸ“œ SIMILAR VOLUMES

Gas chromatography/negative chemical ion
Gas chromatography/negative chemical ionization mass spectrometry of intact glucuronides
✍ Sharon Y. Brown; William A. Garland; Elaine K. Fukuda πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 English βš– 390 KB πŸ‘ 2 views

Gas chromatography-negative chemical ionization mass spectrometry (GC-NCIMS) has been applied to the analysis of 0-and S-glucuronides. The glucuronides were derivatized with pentafluorobenzyl (PFB) bromide and Tri-Sil, and analyzed by GC-NCIMS. All glucuronides gave a large [M-PFBI-ion indicative of