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Gas chromatography and gas chromatography/mass spectrometry for the characterization of complex mixtures of large oligosaccharides

✍ Scribed by Karlsson, H. ;Hansson, G. C.

Publisher
John Wiley and Sons
Year
1988
Tongue
English
Weight
385 KB
Volume
11
Category
Article
ISSN
0935-6304

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✦ Synopsis

High temperature gas chromatography and gas chromatography/mass spectrometry are used in the characterization of complex natural mixtures of permethylated oligosaccharides released from proteins or lipids. The high resolution allows separation of isomeric compounds and the mass range extends to oligosaccharides around molecular mass 2000 daltons or 10 sugar residues for isomalto-oligosaccharides. The mass spectra of permethylated oligosaccharide alditols from mucin glycopeptides are very informative and the approach allows a simple and rapid characterization of these complex components.

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