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Gas chromatographic and mass spectrometric characteristics of 2-trifluoromethyl-3-oxazol-5-ones. A potentially useful derivative for α-amino acids

✍ Scribed by V. Ferrito; R. Borg; J. Eagles; G. R. Fenwick


Publisher
John Wiley and Sons
Year
1979
Tongue
English
Weight
312 KB
Volume
6
Category
Article
ISSN
1076-5174

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✦ Synopsis


The mass spectra of a number of 2-trifluoromethyl-3-oxazol-5-ones, prepared from protein amino acids, have been recorded. The compounds have been separated by gas chromatography using binary column techniques. Analysis of the mass spectra has identified major fragmentation processes which, directly or indirectly, yield the nature of the amino acid sidechain. These fragmentations would be considered advantageous in the identification of unknown a-amino acids.