Gas chromatographic analysis of underivatized tocainide
β Scribed by Joseph M. Scavone; Glenda P. Meneilly; David J. Greenblatt; H. Friedman
- Publisher
- Elsevier Science
- Year
- 1987
- Weight
- 408 KB
- Volume
- 419
- Category
- Article
- ISSN
- 0378-4347
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π SIMILAR VOLUMES
Enantiomer separation of underivatized tocainide and related compounds has been investigated on a column coated with XE-60-L-Val-(S)-a-PEA using ammonia as the mobile phase. No separation was observed when nitrogen or ammonia was initially used as carrier gases. However, after treating the column wi
CP-Sil-5-CB (20 m, 0.25 mm i.d.) 200 "C -O.S"/min ~ 215 "C ' ) CP-Sil-19-CB (25 m, 0.25 mm i.d.) 225 "C -0.2"/min -229 "C ~ 8"/min ~ 261 "C -4"/min -275 "C. dl CP-Sil-5-CB (10 m, 0.25 mm i.d.) CP-Sil-19-CB (10 m, 0.32 mm i.d.) 190 "C ~ l"/min ~ 250 "C. e, CP-Sil-5-CB (10 m. 0.25 mm i.d.) CP-Sil-19-C