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Gallium(III) Iodide-catalyzed Biginelli-type Reaction Under Solvent-free Conditions: Efficient Synthesis of Dihydropyrimidine-2(1H)-one Derivatives

✍ Scribed by Dapeng Li; Haifeng Mao; Litao An; Zhihao Zhao; Prof. Dr. Jianping Zou


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
162 KB
Volume
28
Category
Article
ISSN
0256-7660

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✦ Synopsis


Abstract

The Biginelli‐type condensation of ethyl acetoacetate/cycloketone, aldehyde and urea/thiourea under solvent‐free condition catalyzed by 10% gallium(III) iodide to form dihydropyrimidine‐2(1__H__)‐one derivatives was described. This process offered one way to constructing dihydropyrimidine‐2(1__H__)‐ones in good to excellent yields with simple procedure and short reaction time.


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ChemInform Abstract: Efficient Synthesis
✍ Huihui Zhang; Zhuqing Zhou; Zhigang Yao; Fan Xu; Qi Shen 📂 Article 📅 2009 🏛 John Wiley and Sons ⚖ 29 KB 👁 1 views

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