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Fused oxacycle synthesis via radical cyclization of β-alkoxyacrylates

✍ Scribed by Eun Lee; Jin Sung Tae; You Hoon Chong; Yong Cheol Park; Mikyung Yun; Sangsoo Kim

Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
283 KB
Volume
35
Category
Article
ISSN
0040-4039

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Radical cyclization reaction of a bis(~-alkoxyacrylate) intermediate prepared from (-)-diethyl D-tartrate proceeded stereoselectively to give a 2,6-dioxabicyclo[3.3.0]octane product, which was converted into a known intermediate in the synthesis of kumausallene.