Further Preparation of Substituted 2,6-Bis(2'-pyridyl)pyridines 1
✍ Scribed by CASE, FRANCIS H.; BUTTE, WALTER A.
- Book ID
- 120998164
- Publisher
- American Chemical Society
- Year
- 1961
- Tongue
- English
- Weight
- 565 KB
- Volume
- 26
- Category
- Article
- ISSN
- 0022-3263
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
The crystal structure of the title compound, 2,6-bis[bis(2pyridyl)hydroxymethyl]pyridine, C 27 H 21 N 5 O 2 , at 180 K contains intramolecular OÐHÁ Á ÁN contacts. In space group C2/c, the molecule is sited on a twofold axis.
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.055 wR factor = 0.137 Data-to-parameter ratio = 16.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.009 A Ê Disorder in main residue R factor = 0.068 wR factor = 0.203 Data-to-parameter ratio = 15.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.