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Fungicide Labeling, Preparation of Labeled 2,6-Dichloro-4-nitroaniline (Botran)

✍ Scribed by Groves, Kermit; Robbins, A. L.


Book ID
126120506
Publisher
American Chemical Society
Year
1965
Tongue
English
Weight
240 KB
Volume
13
Category
Article
ISSN
0021-8561

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## Abstract [^14^C] Aniline hydrogen sulphate was acetylated, and the acetanilide obtained was chlorinated with N‐chlorosuccinimide to 2‐chloro, 4‐chloro‐ and 2, 4‐dichloroacet[^14^C] anilide. The labelled 2‐ and 4‐chloroacet[^14^C] anilides were hydrolyzed and treated with aluminium chloride, hydr