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Fundamental studies on extraction of actinides from spent fuels using liquefied gases – Conversion of copper into nitrate with NO2 and extraction of Nd(III) nitrate by CO2 with TBP

✍ Scribed by Kayo Sawada; Daisuke Hirabayashi; Youichi Enokida


Book ID
104087771
Publisher
Elsevier Science
Year
2008
Tongue
English
Weight
476 KB
Volume
50
Category
Article
ISSN
0149-1970

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✦ Synopsis


The nitrate conversion with liquefied NO 2 and the nitrate extraction with SC-CO 2 were demonstrated for copper powder and neodymium nitrate instead of actinide compounds. Copper contacted with NO 2 in an autoclave at 353 K changed to water-soluble compounds. By XRD analysis of the product in the atmospheric condition, the formation of copper nitrate hydrate (Cu(NO 3 ) 2 $2.5H 2 O) was confirmed. As for the extraction, neodymium nitrate loaded in an autoclave was successfully extracted with the fluid of TBP and SC-CO 2 at 15 MPa, 313 K.