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FTIR-Microspectroscopy andDSC Studies of Poly(vinylidene fluoride)

✍ Scribed by Benedetti, Enzo; Catanorchi, Stefano; D’Alessio, Aldo; Moggi, Giovanni; Vergamini, Piergiorgio; Pracella, Mariano; Ciardelli, Francesco

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
491 KB
Volume
41
Category
Article
ISSN
0959-8103

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✦ Synopsis

Poly(viny1idene fluoride) (PVDF) samples, obtained by casting from tetrahydrofuran solutions and submitted to various thermal treatments, have been examined by Fourier transform-infrared microspectroscopy (FTIR-M) and differential scanning calorimetry (DSC). This kind of analysis allowed us to examine microdomains of samples with different morphological characteristics and to obtain an indication of the polymorphism of PVDF. In some cases the simultaneous presence of two or three forms has been evidenced thanks to the comparison of FTIR-M spectra and DSC traces. Vibrational spectra of single crystalline forms can be recorded by FTIR-M on phase homogeneous microdomains.

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