Free radicals in lyophilised food materials
β Scribed by K. A. Munday; M. L. Edwards; G. A. Kerkut
- Publisher
- John Wiley and Sons
- Year
- 1962
- Tongue
- English
- Weight
- 289 KB
- Volume
- 13
- Category
- Article
- ISSN
- 0022-5142
No coin nor oath required. For personal study only.
β¦ Synopsis
Abstract
Food materials dried by the accelerated freeze drying (A.F.D.) process have been tested for free radicals and the concentration and properties of the free radicals compared with those in fresh heart muscle. In fresh muscle at 77Β° K, the freeβradical concentration was between 2.0 and 5.2 Γ 10^15^ per g. of tissue; A.F.D. minced beef 8.28 Γ 10^15^; A.F.D. herring 6.47 Γ 10^14^; A.F.D. maize 1.78 Γ 10^14^; A.F.D. rat cake 1.30 Γ 10^14^. No free radicals were detected in either the minced beef or maize before A.F.D. processing; nor could free radicals be detected in a quickβfrozen (β15Β° c) sample of minced beef stored some weeks. There is a higher concentration of free radicals when the lipid content of the food is high. The freeβradical concentration increased in A.F.D. food in the presence of air and oxygen and also when it was heated to 100Β° c. The addition of water to A.F.D. food reduced the freeβradical concentration to undetectable levels.
π SIMILAR VOLUMES
## Abstract In this work a multiresidual LCβESIβMS/MS method for the simultaneous detection of free and bound fumonisins is described, which allowed for a very low LOD and a very good recovery for all the analytes. The method was applied to the determination of free and bound fumonisins in several