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Free radical fragmentation of photoadduct derivatives leading to allylic systems. Regioselectivity of reduction with tin hydrides and samarium (II) iodide

✍ Scribed by Gordon L. Lange; Christine Gottardo


Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
232 KB
Volume
35
Category
Article
ISSN
0040-4039

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✦ Synopsis


Fragmentation of unsaturated photcadduct derivatives 5 and 8 with (n-Bu)@H, (C,H,),SnH or SmI, generally gives mixtures of regioisomers.

Sml, is the reagent of choice for these transformations because the yields me high (>90%) and with e&xx &t/b only one isomer, Ilalb, is obtained.