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Formation of S-Shaped Disilicoicosatungstate and Efficient Baeyer–Villiger Oxidation with Hydrogen Peroxide

✍ Scribed by Akihiro Yoshida; Masayuki Yoshimura; Kazuhiro Uehara; Shiro Hikichi; Noritaka Mizuno

Publisher: John Wiley and Sons
Year: 2006
Tongue: English
Weight: 151 KB
Volume: 118
Category: Article
ISSN: 0044-8249
DOI: 10.1002/ange.200502543

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## Abstract Silica‐supported propylsulfonic acid is a very good heterogeneous catalyst for the Baeyer–Villiger oxidation of cyclic ketones to lactones with stoichiometric 30% aqueous hydrogen peroxide in 1,1,1,3,3,3‐hexafluoro‐2‐propanol as solvent.