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Formation of monomeric α-butylthioacrolein and its unusual reaction with 2,4-dinitrophenylhydrazine

✍ Scribed by N. A. Keiko; L. G. Stepanova; I. D. Kalikhman; M. G. Voronkov

Book ID
112493691
Publisher
Springer
Year
1977
Tongue
English
Weight
175 KB
Volume
26
Category
Article
ISSN
1573-9171

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Unusual formation of a thiacyclopent-2-e
Unusual formation of a thiacyclopent-2-ene by the reaction of 4,4′-dimethoxythiobenzophenone with tetracyanoethylene
✍ Kentaro Okuma; Yoshikazu Tsujimoto 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 84 KB

## Abstract The reaction of 4,4′‐dimethoxythiobenzophenone (**1a**) with tetracyanoethylene (TCNE) afforded an unusual type of 2:1 adduct with the structure of thiacyclopent‐2‐ene (**5a**). On the other hand, the reaction of thiobenzophenone (**1b**) with TCNE afforded the corresponding thiophene,