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Formation of microheterogeneous film from composite polymer emulsion prepared by the stepwise heterocoagulation method

✍ Scribed by M. Okubo; Y. Lu


Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
201 KB
Volume
69
Category
Article
ISSN
0021-8995

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✦ Synopsis


Blend emulsion of 2 kinds of particles, in which composite polymer particles were prepared by utilizing the stepwise heterocoagulation method proposed by the authors in 1990, was cast to prepare a microheterogeneous film. In the film, a discontinuous phase consisted of large anionic hard polymer particles and a continuous one consisted of small cationic soft polymer particles with the content of 30 wt % as filmforming additives. The storage stabilities of the blend emulsions after the stepwise heterocoagulation were examined under various conditions. The morphology of the film prepared was estimated from attenuated total reflectance Fourier transform infrared spectroscopic and dynamic mechanical spectroscopic measurements.