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Formation of a Stable Sulfenic Acid by Hydrolysis of a Thionitrate and a Sulfenyl Bromide.

✍ Scribed by Kei Goto; Keiichi Shimada; Shunsuke Furukawa; Shinji Miyasaka; Yusuke Takahashi; Takayuki Kawashima

Publisher
John Wiley and Sons
Year
2007
Weight
18 KB
Volume
38
Category
Article
ISSN
0931-7597

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The reaction of ethoxyxcarbonyl isothiocyanate with water isothiocyanate. Compound 2 can be isolated chromatographically, but it is slowly oxidized when allowed to stand in in the absence of a solvent has yielded the new compound [EtO 2 CN=CS 2 C{N(H)CO 2 Et}{S 2 CN(H)CO 2 Et}] (1) in 76% the open a