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Formation of a 1-Azaallenylidene Ligand by Reaction of an Amido Complex with Tetracyanoethylene

✍ Scribed by Morales, Dolores; Pérez, Julio; Riera, Lucía; Riera, Víctor; Miguel, Daniel

Book ID
125942709
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
71 KB
Volume
41
Category
Article
ISSN
0020-1669

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Unusual formation of a thiacyclopent-2-e
Unusual formation of a thiacyclopent-2-ene by the reaction of 4,4′-dimethoxythiobenzophenone with tetracyanoethylene
✍ Kentaro Okuma; Yoshikazu Tsujimoto 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 84 KB

## Abstract The reaction of 4,4′‐dimethoxythiobenzophenone (**1a**) with tetracyanoethylene (TCNE) afforded an unusual type of 2:1 adduct with the structure of thiacyclopent‐2‐ene (**5a**). On the other hand, the reaction of thiobenzophenone (**1b**) with TCNE afforded the corresponding thiophene,