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Formation and structural features of novel cage compounds with a pentacyclo[6.4.0.03,7.04,11.05,10]dodecane skeleton via photolysis of [33](1,3,5)cyclophane

✍ Scribed by Kumi Matohara; Chultack Lim; Mikio Yasutake; Rika Nogita; Toru Koga; Youichi Sakamoto; Teruo Shinmyozu

Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 211 KB
Volume: 41
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)01152-7

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The photolysis of [34](1,2,3,5)cyclophane 5 in H20-saturated CH2Clz produced the novel polycyclic caged diol 6 with a pentacyclo[6.3.1.16,1°.03,7.04,1°]dodecane skeleton 4, which has abnormally elongated C--C single bonds (1.624/k). The structural features of 6 were studied using the X-ray structura