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Formal [4 + 2]-Annulation of Chiral Crotylsilanes: Synthesis of the C19−C28 Fragment of Phorboxazoles

✍ Scribed by Huang, Hongbing; Panek, James S.

Book ID: 125856127
Publisher: American Chemical Society
Year: 2001
Tongue: English
Weight: 62 KB
Volume: 3
Category: Article
ISSN: 1523-7060
DOI: 10.1021/ol015893u

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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The asymmetric synthesis of the spiroketal fragment of mtamycin B is reported employing allylsilane bond construction methodology for the introduction of five of the eight stereogenic centers. In this paper, the construction of the CI9-C28 and C29-C34 fragments as well as their coupling through an a