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Flurbiprofen: Highly potent inhibitor of prostaglandin synthesis

✍ Scribed by Nozu Kaoru

Book ID: 117979801
Publisher: Elsevier Science
Year: 1978
Tongue: English
Weight: 275 KB
Volume: 529
Category: Article
ISSN: 0005-2760
DOI: 10.1016/0005-2760(78)90093-0

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Scheme 1. Synthesis of IFG (1) and IFG derivatives 2-8. a) CH 2 = C(OMe)Me, TsOH•H 2 O, THF, 1.5 h, 0 8C (53 %); b) Tf 2 O, pyridine, CH 2 Cl 2 , 2 h, À78!0 8C; then KCN, 18[crown]-6, DMF, 16 h, RT (80 %); c) RMgX, Et 2 O, 2 h, RT; then NaBH 4 , overnight, RT (65-74 %); d) H 2 , 20 % Pd(OH) 2 /C, Ac