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Fluorine-Containing Organozinc Reagents Part 1 A Simple Synthesis of 2,2-Dichloro-3,3,3-trifluoropropanol

✍ Scribed by Robert Werner Lang

Publisher
John Wiley and Sons
Year
1986
Tongue
German
Weight
329 KB
Volume
69
Category
Article
ISSN
0018-019X

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## Abstract A synthetic route for obtaining 1‐butoxy‐1,3,3‐triethoxy[1,3‐^2^H~2~]propane a stable diacetal of the malondialdehyde, is described. The synthesis involves the condensation of deuterated butylvinyl ether with deuterated triethyl orthoformate in the presence of montmorillonite clay K‐10.