Flow-injection Fourier transform infrared spectrometric analysis
β Scribed by M. de la Guardia; S. Garrigues; M. Gallignani; J.L. Burguera; M. Burguera
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 421 KB
- Volume
- 261
- Category
- Article
- ISSN
- 0003-2670
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β¦ Synopsis
A method has been developed for obtammg and stormg the complete Fourier transform spectrum, of a sample m a flowmg stream m only 19 s A resolution of 4 cm-l IS recommended The determmahon of o-xylene m xylol was employed as a test system, usmg hexane as a tamer and dduent m all the expenments A classlcal hqmd flow cell and a demountable flow-through cell were compared The best hmlt of detectlon obtamed was 0 01% (v/v) The effects of flow-rate and lnjectlon volume were studled for the two cells used The relative standard devlatlon (0 4% o-xylene, n = 5) was ca 1%
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