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Flow-injection Fourier transform infrared spectrometric analysis

✍ Scribed by M. de la Guardia; S. Garrigues; M. Gallignani; J.L. Burguera; M. Burguera


Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
421 KB
Volume
261
Category
Article
ISSN
0003-2670

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✦ Synopsis


A method has been developed for obtammg and stormg the complete Fourier transform spectrum, of a sample m a flowmg stream m only 19 s A resolution of 4 cm-l IS recommended The determmahon of o-xylene m xylol was employed as a test system, usmg hexane as a tamer and dduent m all the expenments A classlcal hqmd flow cell and a demountable flow-through cell were compared The best hmlt of detectlon obtamed was 0 01% (v/v) The effects of flow-rate and lnjectlon volume were studled for the two cells used The relative standard devlatlon (0 4% o-xylene, n = 5) was ca 1%


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