Boron as boric acid was determined with chromotropic acid using a fluorescence detection-flow injection system. The flow system consisted of three streams, a carrier, a reagent and an alkaline solution. By mixing 0.5 M sodium hydroxide solution as the alkaline solution, the high background fluoresce
Flow-injection determination of sulphonamides with fluorimetric or photochemical-fluorimetric detection
โ Scribed by M.C. Mahedero; J.J. Aaron
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 413 KB
- Volume
- 269
- Category
- Article
- ISSN
- 0003-2670
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โฆ Synopsis
A flow-mJectlon method with photochemlcally Induced fluorescence (PF) or native fluorescence (NF) detectlon was developed for the determmatlon of four sulphonamldes Sulphamethazme was determmed usmg PF and sulphamlamtde, sulphaguamdme and sulphacetanude using NF Linear cahbratlon graphs were obtamed over a concentration range of one order of magnitude The relative standard devlatlons were within the range 04-5% Lmuts of detection were between 0 015 and 0 12 pg ml-' The method was apphed to the determmatlon of sulphonamides m mdk and pharmaceutical preparations
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