A new chromatographic system for the simultaneous analysis of polyethylene glycol, dextran, sugars, and low-molecular-weight fatty acids was developed. The system is based on a gel exclusion column which allows a first separation between high-and lowmolecular-weight compounds, and a cationic exchang
Flooding characteristics of aqueous two-phase systems in a countercurrent sieve-plate column
β Scribed by Ahd Hamidi; Mos van Berlo; Karel ChAM Luyben; Luuk AM van der Wielen
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1999
- Tongue
- English
- Weight
- 132 KB
- Volume
- 74
- Category
- Article
- ISSN
- 0268-2575
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β¦ Synopsis
The hydraulic capacity of countercurrent liquid-liquid extractors is constrained by its Γ½ooding characteristics. This study presents Γ½ooding data for aqueous two-phase systems containing PEG 4000 and at various concentrations in a countercurrently operated sieve-plate column in Na 2 SO 4 the absence of solutes. Flooding limits, average droplet sizes and dispersed phase hold-ups at Γ½ooding conditions were measured as well as densities, interfacial tensions and viscosities. A correlation proposed by Richardson and Zaki (Trans IChemE 32 :35-53 (1954)) was used successfully for the description of the slip velocities and thus maximum column throughputs. 1999 Society of Chemical Industry
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