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Fischer indole synthesis from cis- and trans-9-methyl-3-decalone

✍ Scribed by Miller, F. M.; Lohr, Raymond A.

Book ID: 127372396
Publisher: American Chemical Society
Year: 1978
Tongue: English
Weight: 228 KB
Volume: 43
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00411a027

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## Abstract A method is described for the synthesis of the racemic [methyl‐d~3~] forms of the nicotine metabolites __cis__‐3′‐hydroxycotinine and __trans__‐3′‐hydroxycotinine. The key intermediate was [methyl‐d~3~]‐N‐methylhydroxylamine, obtained from a selective hydrogenation of d~3~‐nitro‐methane