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First total synthesis of macrosphelides C and F

✍ Scribed by Yuichi Kobayashi; Hukum P Acharya

Book ID
104230358
Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
71 KB
Volume
42
Category
Article
ISSN
0040-4039

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✦ Synopsis

Macrosphelides C and F were synthesized by lactonization of 14-oxo seco acids at the O(10) C( ) bond followed by reduction and Mitsunobu inversion of the resulting hydroxyl group. The seco acids were prepared from the corresponding furans by furan ring-opening with NBS followed by further oxidation of the 4-oxo-2-alkenals with NaClO 2 .

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ChemInform Abstract: First Total Synthes
ChemInform Abstract: First Total Synthesis of Macrosphelides C and F.
✍ Yuichi Kobayashi; Hukum P. Acharya πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 28 KB πŸ‘ 2 views

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