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Far infrared study of iron(II) and copper(II) coordination compounds with 4,4′-didodecyloxy-2,2′-bipyridine and 4,4′-dioctadecyloxy-2,2′-bipyridine

✍ Scribed by Andrzej T. Kowal; Jacek Skarzewski

Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
381 KB
Volume
41
Category
Article
ISSN
1386-1425

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✦ Synopsis

Novel coordination compounds of the type Fe(LC,,)&, Fe(LC,s)sCla, Cu(LC,,)CI, and Cu(LC,s)Cla (where LCia and LCis denote 4,4'-didodecyloxy-2,2'-bipyridine and 4,4'-dioctadecyloxy-2,2'bipyridine, respectively) have been synthesized and characterized by means of their far i.r. spectra. On the basis of 63Cu-65Cu and s4Fes6Fe isotope substitutions the assignments of bands due to metal-ligand vibrations have been made. A pseudooctahedral (0s) structure has been proposed for both iron(H) comnlexes, whereas a polymeric octahedral, chloride bridged structure (Ci) seems most favorable for both cop&II) complexes. _ _

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