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Facile synthesis of (4S)-(−)-[9-3H]limonene

✍ Scribed by Yoshikazu Hiraga; Hiroshi Danjo; Takatoshi Ito; Takayuki Suga

Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
236 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

(4__S__)‐[9‐^3^H]‐1‐Methyl‐4‐(1′‐methylethenyl)cyclohexene ((4__S__)‐(−)‐[9‐^3^H]limonene) was synthesized from (1′S,2__RS__)‐2‐(4′‐methylcyclohex‐3′‐enyl)porpanal ((4__S__,8__RS__)‐(−)‐1‐p‐menthen‐9‐al) via a convenient route in a high yield with improved enantiomeric purity.

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