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Facile Synthesis of 2-Alkylthio-5,6,7,8-tetrahydrobenzothieno[2,3- d ]pyrimidin-4(3 H )-ones

✍ Scribed by Zeng, Xiao-Hua; Liu, Min; Ding, Ming-Wu; He, Hong-Wu


Book ID
120244597
Publisher
Taylor and Francis Group
Year
2010
Tongue
English
Weight
199 KB
Volume
40
Category
Article
ISSN
0039-7911

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## Abstract magnified image The thienopyridine derivative **2**, obtained from reaction of acetoacetic ester with **1** in the presence of tin tetrachloride, was treated with triphenylphosphine in hexachloroethane and Et~3~N to give iminophosphorane **3**. Iminophosphorane **3** reacted with pheny