Facile Synthesis of 2-Alkylthio-5,6,7,8-tetrahydrobenzothieno[2,3- d ]pyrimidin-4(3 H )-ones
β Scribed by Zeng, Xiao-Hua; Liu, Min; Ding, Ming-Wu; He, Hong-Wu
- Book ID
- 120244597
- Publisher
- Taylor and Francis Group
- Year
- 2010
- Tongue
- English
- Weight
- 199 KB
- Volume
- 40
- Category
- Article
- ISSN
- 0039-7911
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π SIMILAR VOLUMES
In the title molecule, C 18 H 25 N 3 O 2 S, the central thienopyrimidine ring system is essentially planar. The cyclohexene ring, in which the four CH 2 groups are disordered in an approximately 1:1 ratio, adopts a half-chair conformation, while the morpholine ring is in a standard chair conformatio
In the title compound, C~19~H~27~N~3~OS, the central thienopyrimidine ring system is essentially planar. The cyclohexene ring adopts a half-chair conformation, while the piperidine ring is in a standard chair conformation. There is an intramolecular CβH...O hydrogen bond, which stabilizes the molecu
## Abstract magnified image The thienopyridine derivative **2**, obtained from reaction of acetoacetic ester with **1** in the presence of tin tetrachloride, was treated with triphenylphosphine in hexachloroethane and Et~3~N to give iminophosphorane **3**. Iminophosphorane **3** reacted with pheny