✦ LIBER ✦

Facile synthesis of 1-nitropyrene-d9 of high isotopic purity

✍ Scribed by Alexander J. Fatiadi; Laurence R. Hilpert

Book ID: 102371011
Publisher: John Wiley and Sons
Year: 1989
Tongue: French
Weight: 318 KB
Volume: 27
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580270203

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✦ Synopsis

dinitropyrene-d,, used as internal standards for the determination of nitropolycyclic aromatic hydrocarbons (NPAH) in simple and complex mixtures, and required for GC/MS measurements used in the certification of NBS Standard Reference Material (SRM) 1596 (a mixture of nitropyrenes), were synthesized in one step from commercially available pyrene-dlo and nitric acid-gl. The electron impact mass spectra and isotopic purity of 1-nitropyrene-d, and the deuterated dinitropyrenes were determined; the compounds were characterized by gas chromatography-mass spectrometry (GC-MS) and by high performance liquid chromatography (HPLC).

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