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Facile Preparation and Reactivity of Magnetic Nanoparticle- Supported Hypervalent Iodine Reagent: A Convenient Recyclable Reagent for Oxidation

✍ Scribed by Chenjie Zhu; Yunyang Wei

Publisher: John Wiley and Sons
Year: 2012
Tongue: English
Weight: 703 KB
Volume: 354
Category: Article
ISSN: 1615-4150
DOI: 10.1002/adsc.201100601

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✦ Synopsis

Abstract

A simple three‐step preparation of magnetic nanoparticle‐supported (diacetoxyiodo)benzene starting from 4‐iodobenzoic acid is described. The nanoparticle reagent was obtained with good loading levels and has been successfully used for efficient oxidation of a wide range of alcohols. The supported reagent demonstrated comparable activity with that of its homogeneous counterpart (diacetoxyiodo)benzene and could be simply recycled with the assistance of an external magnet.

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