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Facile one-step synthesis of a thia-bridged bis-1,10-phenanthroline macrocycle

✍ Scribed by Wen-Jwu Wang; Abdurrahman Sengul; Chi-Feng Luo; Hsien-Chang Kao; Yi-Hung Cheng

Book ID: 104254296
Publisher: Elsevier Science
Year: 2003
Tongue: French
Weight: 83 KB
Volume: 44
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(03)01710-6

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✦ Synopsis

An efficient one-pot synthesis of a macrocyclic ligand, consisting of two 1,10-phenanthroline nuclei bridged by sulfur, is described. A spectrophotometric investigation reveals the isolated compound to be the mono-trifluoroacetate salt. Symmetrical NH-and S-bridged tetradentate ligands were also synthesized by the new method.

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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