Dichloromethane and acetonitrile containing thiophene and oxidant, respectively, were adopted as a binary organic solvent for oxidative synthesis of unsubstituted polythiophene (UPTh) under various conditions, i.e., oxidant/monomer molar ratio, polymerization temperature, and reaction time. We also
β¦ LIBER β¦
Facile High-Yield Synthesis of Polyaniline Nanosticks with Intrinsic Stability and Electrical Conductivity
β Scribed by Xin-Gui Li; Ang Li; Mei-Rong Huang
- Publisher
- John Wiley and Sons
- Year
- 2008
- Tongue
- English
- Weight
- 603 KB
- Volume
- 14
- Category
- Article
- ISSN
- 0947-6539
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## Abstract A wholly aromatic polypyrene was synthesized by direct chemical oxidative polymerization of pyrene with ferric chloride as oxidant in hexane/nitromethane. Successful synthesis of polypyrene was thoroughly confirmed by IR, UV/Vis, 1D ^1^Hβ NMR, 2D ^1^Hβ^1^H COSY, 2D ^1^Hβ^13^C HSQC, MALDI
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