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Facile and efficient sonochemical synthesis of 1,4-disubstituted 1,2,3-triazole derivatives catalyzed by CuI under mild conditions

✍ Scribed by Naeimi, Hossein; Dadashzadeh, Samira; Moradian, Mohsen


Book ID
121625797
Publisher
Springer Netherlands
Year
2013
Tongue
English
Weight
278 KB
Volume
41
Category
Article
ISSN
0922-6168

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Ph TBSO(CH 2 ) 3 THPO(CH 2 ) 2 THPOCH 2 TBSOCH 2 n-C 4 H 9 R 1) 1 equiv n-BuLi; THF; -40 ΒΊC 2) 2 equiv DMF; -40 ΒΊC to r.t.; 0.5h 3) "Reverse" 10% aq. KH 2 PO 4 (4 equiv); MTBE; 5 ΒΊC (Ref. 9) 1 2 (a) (a) Position of the triazole NH is arbitrarily assigned since we cannot differentiate reliably betwee