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fac-Tricarbonyltris(triphenyl phosphite)molybdenum(0)

✍ Scribed by Alyea, E. C. ;Ferguson, G. ;Song, S. Q.

Book ID
114512232
Publisher
International Union of Crystallography
Year
1995
Tongue
English
Weight
582 KB
Volume
51
Category
Article
ISSN
0108-2701

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fac-Tris(tert-butyl isocyanide)tricarbon
fac-Tris(tert-butyl isocyanide)tricarbonylΒ­molybdenum(0)
✍ Imhof, Wolfgang ;Halbauer, Kathi ;DΓΆnnecke, Daniel ;GΓΆrls, Helmar πŸ“‚ Article πŸ“… 2006 πŸ› International Union of Crystallography 🌐 English βš– 182 KB

The title compound, [Mo(C 5 H 9 N) 3 (CO) 3 ], was produced from Mo(CO) 6 and tert-butyl isocyanide in the presence of 10 atm of carbon monoxide (1 atm = 101325 Pa). The octahedral complex shows a facial arrangement of the ligands, the Mo-C distances of the isocyanide ligands being about 0.15 A ˚lon