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Fabrication of nanocrystalline ZnWO4 with different morphologies and sizes via hydrothermal route

✍ Scribed by Shu-Jian Chen; Jian-Hao Zhou; Xue-Tai Chen; Jing Li; Li-Hong Li; Jian-Ming Hong; Ziling Xue; Xiao-Zeng You


Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
282 KB
Volume
375
Category
Article
ISSN
0009-2614

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✦ Synopsis


ZnWO 4 nanocrystals have been prepared via a hydrothermal route, and characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), and X-ray photoelectron spectroscopy. The size and morphology of ZnWO 4 nanocrystals were found to depend on the reaction temperature and pH. The length of ZnWO 4 nanorod increased with the increase in pH of the hydrothermal solution. An unusual nanoparticle-to-nanorod transformation was observed during the formation of ZnWO 4 nanoparticles at pH 11.0 and 180 °C. Luminescent properties of ZnWO 4 nanocrystals were investigated by photoluminescence (PL) spectroscopy.


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2D and 3D nano/microstructures of 4ZnO•B 2 O 3 •H 2 O with different morphologies have been successfully synthesized by a hydrothermal route in the presence of surfactant polyethylene glycol-300 (PEG-300). Lamellar-like nanoparticles and microsphere organizations of nano and microrods are fabricated