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Extraction catalytic determination of copper in non-aqueous medium

✍ Scribed by Otto, M. ;Bontchev, P. R. ;M�ller, H.

Publisher
Springer-Verlag
Year
1977
Weight
494 KB
Volume
67
Category
Article
ISSN
0344-838X

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Determination of trace vanadium in organic solvents is studied by use of the oxidation of o-dianisidine with t-butyl hydroperoxide. The sensitivity of the catalyzed reaction is optimized by application of a modified simplex method. Under optimum conditions the detection limit is 0.7 ng V I&' in acet