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Exploring potential energy hypersurfaces for triple symmetric inversion in 3-azabicyclo[3.3.1]nonan-9-one and itsN-methyl derivative

✍ Scribed by Smeyers, N. J.; Melendez, F. J.; Smeyers, Y. G.


Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
298 KB
Volume
19
Category
Article
ISSN
0192-8651

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✦ Synopsis


The potential energy hypersurfaces for the triple inversion, from chair to boat and ␣ to ␤ conformations, are explored theoretically in 3w x azabicyclo 3.3.1 nonan-9-one and its N-methyl derivative, by using ab initio quantum-mechanical calculations. Both compounds are precursors of rigid analogs of the potential GABA and GABA receptor antagonists. In contrast to

results from semiempirical calculations, the chair᎐chair ␤ conformers are found to be, by far, the most stable structures for both the nonmethylated and N-methylated compounds. The inversion barriers are found to be relatively low, so that the conformers could be expected to exist in thermodynamic equilibrium at room temperature. A population analysis reveals, however, that, in the ab initio approach, the molecules seem to exist practically only in the chair᎐chair᎐␤ conformation. The theoretical results compare well with the available experimental data.