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Experiments with the PTV in the solvent split mode for concentration of volatiles

โœ Scribed by Villen, J. ;Herraiz, T. ;Reglero, G. ;Herraiz, M.

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
301 KB
Volume
12
Category
Article
ISSN
0935-6304

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Sampling of volatile components using a
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Several packing materials were evaluated for their sampling performance with a cold programmed temperature vaporizing injector operated in the solvent split (solvent elimination) mode. Evaluations were made by comparing accuracy and precision of the data for mixtures of n-alkanes, ethyl esters, n-al

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In this study, the cold split-splitless injector recently introduced by Carlo Erba was optimized for the trace analysis of polycyclic aromatic hydrocarbons. Injections of hundreds of microliters of hexanesolutions were performed in the solvent split mode using an autosampler programmed for large vol