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Experimental and theoretical study of two novel thioperoxides: Methoxycarbonylsulfenyl acetate, CH3OC(O)SOC(O)CH3, and methoxycarbonylsulfenyl trifluoroacetate, CH3OC(O)SOC(O)CF3

✍ Scribed by Lin Du; Li Yao; Xiao-Qing Zeng; Mao-Fa Ge

Publisher
Elsevier Science
Year
2008
Tongue
English
Weight
400 KB
Volume
876
Category
Article
ISSN
0022-2860

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Pure N,N 0 -di(methoxycarbonylsulfenyl)urea, [CH 3 OC(O)SNH] 2 CO, is quantitatively prepared by the hydrolysis reaction of CH 3 OC(O)SNCO and characterized by 1 H NMR, GC-MS and FTIR spectroscopy techniques. Structural and conformational properties are analyzed using a combined approach with data o