𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Experimental and Computational Study on a Variety of Structural Motifs and Coordination Modes in Aluminium Complexes of Di(2-pyridyl)amides and -phosphanides

✍ Scribed by Matthias Pfeiffer; Alexander Murso; Lepakshaiah Mahalakshmi; Damien Moigno; Wolfgang Kiefer; Dietmar Stalke


Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
363 KB
Volume
2002
Category
Article
ISSN
1434-1948

No coin nor oath required. For personal study only.

✦ Synopsis


N ligands / P ligands

The (2-Py) 2 N -ligand shows much more conformational freedom than the (2-Py) 2 P -anion in aluminium coordination. The two isomers [Al{(NPy)Py} 3 ] (1a) and [Al{(NPy)Py} 2 (Py 2 N)] (1b) were isolated, the former containing exclusively cistrans ligands, and the latter cis-trans ligands together with a trans-trans ligand. The energy differences in the noncoordinated anions (2-Py) 2 E -(E = N, P) were determined by computational methods to be low in the amide. While the NǞAl