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Excretion products of algae: Identification of biogenic amines by gas-liquid chromatography and mass spectrometry of their trifluoroacetamides

✍ Scribed by V. Herrmann; F. Jüttner

Publisher
Elsevier Science
Year
1977
Tongue
English
Weight
477 KB
Volume
78
Category
Article
ISSN
0003-2697

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✦ Synopsis

The trifluoroacetyl derivatives of 12 biogenic amines were separated by gas-liquid chromatography and identified by mass spectrometry. Vacuum sublimation was used to separate nanomole quantities of amines from algal media and natural waters that contained algae. Trimethylamine, I-aminopropane, 2-aminopropane, and ethanolamine were found in the culture medium of Ochromonas.

Chlamydomonas-enriched backwater contained butanolamine. I-Aminopropane was found in the media of Nitzschia, Ankistrodesmus.

and Microcystis.

Concentrations were approximately 300 pg/liter for Ankistrodesmus and 240 pg/liter for Microcystis media.

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