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Evolution of grain shape and size during high-temperature creep of a yttria-doped fine-grained alumina

✍ Scribed by P. Gruffel; F. Righetti; C. Carry


Publisher
Springer
Year
1993
Tongue
English
Weight
658 KB
Volume
28
Category
Article
ISSN
0022-2461

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✦ Synopsis


A semi-automatic method of image analysis was used to characterize the evolution of the microstructure of a polycrystalline alumina in terms of grain size and grain shape during different thermomechanical treatments. This study showed that for this material normal grain growth occurs during compressive creep and annealing; in addition, during creep under certain conditions grains flatten in the direction of the applied stress. Three-dimensional estimation of the grain shape was performed by analysing differently oriented plane sections of the specimens.


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The high temperature mechanical behaviour of 4% mol yttria tetragonal zirconia polycrystals (4-YTZP) with different grain sizes (0.38 < d < 1.15 m) has been analyzed by means of compression creep tests. The working temperature was 1350 • C and the strain rates ranged between 5 × 10 -7 and 2 × 10 -4