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Evidence for the occurrence of an oxygen to oxygen acyl shift in 7-acetoxybicyclo|3,2,0|heptan-2-ones upon chemical ionization mass spectrometry

✍ Scribed by Magda Claeys; Martine van Audenhove; Maurits Vandewalle


Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
231 KB
Volume
88
Category
Article
ISSN
0037-9646

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✦ Synopsis


Abstract

An oxygen to oxygen acyl migration has been observed in 7‐acetoxybicyclo|3,2,0|heptan‐2‐ones upon isobutane chemical ionization mass spectrometry. The mechanism of this rearrangement is discussed and is investigated by means of deuterium labelling techniques.