Evaluation of degree of hydration in concrete using 29Si magic angle spinning NMR in solids
β Scribed by G. Parry-Jones; A.J. Al-Tayyib; A.I. Al-Mana
- Publisher
- Elsevier Science
- Year
- 1988
- Tongue
- English
- Weight
- 231 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0008-8846
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β¦ Synopsis
The degree of hydration of cement and concrete can be followed using 29Si MAS-NMR. Preliminary results of the effects of hydration on the distribution of silicate polymers in concretes of known mix designs, as well as the constituent cement, are presented. The spectra of the sand and aggregate used are also given. The technique appears promising as a means of monitoring concrete silicate anion structure and its possible correlation with mechanical properties.
π SIMILAR VOLUMES
Hydration of RPC (Reactive Powder Concrete) and pozzolanic reaction were studied by zgSi NMR using SPE/MAS technique. Industrial cement and materials (silica fume, crushed quartz) constitutive of RPC imposed a careful study of spectra acquisition (relaxation times, spinning velocity). + . . Two RPC
29 Si magic angle spinning (MAS) NMR, 27 Al MAS NMR and 27 Al triple-quantum MAS NMR were used to study the dealumination of offretite occurring during hydrothermal treatment. Deformed tetrahedral ( Si-O-) 3 Al-OH species and two octahedral extra-framework species are formed during the course of th