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Evaluation of amberlite xad-2 as the extractant for carbmate insecticides from natural water

✍ Scribed by K.M.S. Sundaram; S.Y. Szeto; R. Hindle

Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
436 KB
Volume
177
Category
Article
ISSN
1873-3778

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✦ Synopsis

A rapid and sensitive analytical technique to quantify carbamate insecticides at nanogram levels is reported using resin column and sorption, and desorption followed by N-P gas-liquid chromatography (GLC) analysis. The carbamates were extracted from natural water by percolation through a column of Amberlite XAD-2, followed by elution with ethyl acetate. The carbamate residues were directly analyzed by GLC with a Tracor Model 702 N-P detector. The recoveries for several carbamates including aminocarb, mexacarbate, carbaryl, propoxur, carbofuran, pirimicarb and methiocarb were from 86 to 108% at 1.0 and 0.01 ppm levels. Only 41 to 58% was recovered for methomyl. The extraction efficiency of Amberlite XAD-2 was pH-dependent as indicated in the extraction of aminocarb. More than 90% of the added aminocarb was recovered from phosphate buffer by the described method at pH 5.0 to 7.5 at 5.0 and 0.5 ppm levels.

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