The use of predictive models for the understanding and management of sediment and contaminant transport generally requires knowledge of particle size and settling velocity. Particle size is often obtained by direct measurements, and the settling velocities are usually predicted using the Stokes' law (or a modification thereof) for single-grained spherical particles. Such measurements and estimates are not satisfactory measures for cohesive sediments, which exist as agglomerated particles called flocs and whose behaviour is significantly different from that of the singlegrained particles. Direct measurement of settling velocity and size using optical methods in settling columns has also been employed to improve these predictions; however, the subjectivity in determining which particles are in focus results in unreliable size data. An out-of-focus particle will generally possess a larger size than in reality. This paper evaluates a laser-assisted particle sizing/settling velocity determination technique's ability to eliminate the subjectivity and improve particle-sizing accuracy during settling column experiments. Although the diffraction of light by the translucent standard beads (used for evaluating the technique's accuracy for determining particle size) posed a problem, the results suggest that this technique has potential for assisting researchers to obtain the most accurate settling particle size data possible.