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Evaluation of a fluorocarbon bonded silica using packed capillary column supercritical fluid chromatography

✍ Scribed by Wenbao Li; Elena Ibaňez; Abdul Malik; Milton L. Lee

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
685 KB
Volume
8
Category
Article
ISSN
1040-7685

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✦ Synopsis

A newly commercialized fluorinated silica, Fluofix 120N

[1H71H,2H,2H,3H,3H-tridecafluord4,4-dimethy1hepty1)si1y1 bonded spherical microporous silica gel], was used as a packing material for supercritical fluid chromatography (SFC). The performance and stability of this fluorinated phase were examined under different experimental conditions. The SFC behavior of this phase was compared with a conventional C,, bonded reversed phase. The excellent separation power of the Fluofix 120N phase for fluorinated compounds was demonstrated by high-resolution separations of different perfluorinated polymers.

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