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Ethylene-Bridged Tetramethylcyclopentadienylamide Titanium Complexes: Ligand Synthesis and Olefin Polymerization Properties †

✍ Scribed by van Leusen, Daan; Beetstra, Dirk J.; Hessen, Bart; Teuben, Jan H.

Book ID
126102503
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
100 KB
Volume
19
Category
Article
ISSN
0276-7333

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✍ Zofia Janas; Lucjan B. Jerzykiewicz; Katarzyna Przybylak; Piotr Sobota; Krzyszto 📂 Article 📅 2004 🏛 John Wiley and Sons 🌐 English ⚖ 155 KB

## Abstract The mixed‐ligand complexes [Ti~2~(μ‐OR)~2~(OR)~2~(κ^3^‐tbop)~2~] (1a) for R = Me and (1b) R = Et were prepared by the reaction of Ti(OR)~4~ and H~2~tbop {H~2~tbop = 2,2′‐thiobis[4‐(1,1,3,3‐tetramethylbutyl)phenol]} in methanol. Treatment of 1a and 1b with AlMe~3~ led to the substitution