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Ethyl 6-methoxy-2-naphthoate

✍ Scribed by Yathirajan, H. S. ;Bindya, S. ;Sarojini, B. K. ;Narayana, B. ;Bolte, Michael

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 313 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807017977

No coin nor oath required. For personal study only.

✦ Synopsis

A sample of ethyl 6-methoxy-2-naphthoate was obtained from Strides Arco Labs, Mangalore, India. Colourless plates of (I) were obtained by slow evaporation using a mixture (1:1 v/v) of acetone and toluene (m.p.: 359-361 K).

Refinement

The H atoms were found in a difference map, relocated in idelised loations (C-H = 0.95-0.99 Å), and refined as riding with U iso (H) = 1.2U eq (C) or U iso (H) = 1.5U eq (C methyl ). The methyl groups were allowed to rotate but not to tip.

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